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BTA 2100D
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Axis BTA 2100D Manual del operador Pagina 318
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316
GC.
Bunch Size
Displays the data acquisition bunch size.
Freq
Displays the data acquisition bunch rate, in Hz.
1
2
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596
597
Operation Manual
1
Contents
3
Getting Started
13
MS Workstation Toolbar
15
Button
16
Application Buttons
17
Quick Link Buttons
18
Move to Windows Taskbar
24
Application Descriptions
25
Small Buttons on Toolbar
25
2000 MS Module Control
27
Network
30
Company Network)
34
Server]
35
Click Setup
35
2000 MS Instrument Control
49
2000 Module Window
50
Manual Control
51
Instrument Settings
52
Setpoints tab
52
Adjustments tab
52
Auto Tune
53
Set Points
54
Temperatures
55
Diagnostics Mode
55
System Test
56
Monitor Window
57
Shutdown Mode
58
Acquisition Mode
59
2000 MS Instrument Window
61
Inject Single Sample Menu
64
Saturn Module Keypad Dialog
71
Spectrum Toolbar
72
Status and Control Window
75
Operating Conditions
77
SetPoints
77
Adjustments
78
See the Chemical Ionization
81
Autotune Mode
82
Control and Status
83
Method and Set Points
83
Auto Tune Checks
85
Air/Water Check
85
Electron Multiplier Tune
86
Mass Calibration
88
Trap Function Calibration
89
Temperatures Mode
90
Diffusion Pump Shutdown
94
Diffusion Pump Startup
95
Acquisition
96
Electron Multiplier Gain
98
Axial Modulation
99
Emission Current
99
Ion Trap Temperature
99
AGC Target TIC Value
100
The Instrument Window
101
Overview
109
Specifying a RecalcList
112
Using QuickStart
113
3800 GC Injecting Multiple
115
Samples
115
Using the Sequence Window
122
Adjust time scale
130
Select Edit Module Info
131
3900 GC Injecting Multiple
139
System Control Menus
147
Edit Menu
148
Inject Menu
149
Automation Menu
149
Recalculate Menu
150
Instrument Menu
150
Windows Menu
151
Help Menu
152
System Control Toolbar
153
2000 MS Method Basic Scan
155
Functions
155
2000 MS Method Chemical
157
Ionization
157
The CI Parameters
160
Ejection Amplitude (v)
161
Background mass
161
Target TIC Value
161
Maximum ionization time
161
Maximum reaction time
161
Prescan Ionization Time
162
Using Liquid CI Reagents
164
Choice of Liquid CI Reagents
165
Than Methane
167
Tuning for CI Operation
168
Recommended Reading
169
2000 MS Method Command
171
Reference
171
The flow sampling segment
172
Ionization Mode
173
Ion Preparation
173
Segment Setpoints
174
Ionization Mode - EI Auto
175
Ionization Mode - EI Fixed
176
CI Fixed Parameters
178
Ion Storage (SIS) Parameters
179
Customize SIS
179
The MS/MS Ion Prep Method
180
Item Description
181
Customize Resonant Method
182
Ion Preparation MS/MS
185
2000 MS Method Electron
191
Ion Formation
192
AGC Prescan
192
Mass Scanning
193
Software Parameters
195
Mass Range Segment Breaks
197
Ionization Storage Level
197
Ionization Time Factor
197
Maximum Ionization Time
198
Background Mass
198
The Ion Preparation Method
201
Autoscale Waveform
206
Tips for Using SIS
207
Theory of Operation
209
Parent Ion Isolation
210
Product Ion Formation
210
Product Ion Mass Scanning
213
Chemical Ionization
213
Control
213
Summary
213
The MS “q” Calculator
216
Isolation
217
Dissociation
220
Excitation amplitude (volts)
224
Parent ion
224
Product ion 1
224
Product ion 2
224
Using Nonresonant Excitation
225
MS/MS/MS
226
2000 MS Method Section
229
The Method Builder Window
232
The 2000 MS Method Windows
233
The Flow Sampling Segment
235
The Startup Method
237
Status Window
238
Importing Method Sections
239
Deleting Method Sections
240
Printing the Method
241
Password Protecting a Method
241
3800 GC Method Command
243
Default Clean Section
244
Clean Mode Section
245
Internal Standard Section
246
Solvent Plug Settings
247
User Defined Settings
248
Viscosity Settings
248
3800 GC Sample Delivery
250
3800 GC Injector
251
1061 Injector
252
1079 Injector
252
Spilt Ratio Dialog Box
253
3800 GC Flow/Pressure
255
Type 4 (for valved systems)
257
3800 GC Column Oven
258
3800 GC Detector
259
FID Detector
260
TCD Detector
261
TSD Detector
262
ECD Detector
264
PFPD Detector
265
Methanizer Dialog Box
266
3800 GC Output
267
3800 GC Data Acquisition
268
3800 GC Method Section
269
MS Workstation
270
The 3800 GC Method Windows
273
Spreadsheet editing
274
Checking Method End times
275
Sample Delivery Window
276
Injector Window
278
1177 Injector
280
1041 Injector
281
SPT Injection Device
282
Flow/Pressure Window
283
Pressure spreadsheet
286
Flow spreadsheet
286
Column Oven Window
287
Detector Window
288
Micro-TCD Detector
292
Output Window
296
Data Acquisition Window
297
Autosampler Window
298
Hardware
299
3800 GC System Control
305
Command Reference
305
3800 Operation Display
306
Temp Zones Status Display
307
Component Status Display
307
Column Oven Status:
308
AutoSampler Status:
309
Sample Delivery Status:
310
Name Default State Energized
310
1041/1061 Injector Status:
312
SPT Injector Status:
313
FID Status:
317
ECD Status:
319
TSD Status:
319
PFPD Status:
320
8400/8410 Carrousel Display
324
Chromatogram Display Toolbar
325
3800 Setup Dialog Box
326
Field Description
328
3900 GC Method Command
335
3900 GC Injector Section
343
Type 1 (for 1177 injector)
345
3900 GC Column Oven Section
346
3900 GC Method Section
347
The 3900 GC Method Windows
351
GC Control Window
354
Injector Section
355
Column Oven Section
357
3900 GC System Control
365
Oven Status Display
367
Injector EFC Status Display
368
3900 Setup Dialog Box
369
8200 AutoSampler Instrument
383
Control Command Reference
383
Hardware Dialog Box
386
Automix Routines Dialog Box
387
Carrousel Dialog Box
389
8200 Configuration Window
391
Liquid Sampling Options
392
User Defined Parameters
393
SPME Options
394
Main Toolbar
399
Print Setup Dialog Box
402
Edit Notes Dialog Box
403
RecalcList Window
404
Open Data File Dialog Box
409
SampleList Window
410
Sequence Window
416
Automation File Editor
417
GC Batch Report
427
Method Selection
428
Generating Reports
429
Changing Report Commands
429
GC Data Handling Calibration
431
Automated Calibration
432
Select View Curves
435
Calibration Verification
436
Introduction
437
Performing a Pilot Run
437
Peak Detection
438
Rejecting Solvent Peaks
439
Skimming Fused Peaks
439
Splitting Fused Peaks
440
Forcing Peaks
440
Identifying Peaks
441
Building a Calibration Curve
441
Choosing a Calibration Type
443
GC Data Handling Method
445
Peak Table
447
Calibration Setup
449
Coefficients Table
451
Calibration Curve Window
452
This Report Only Dialog Box
453
Print All Dialog Box
454
Overlay Window
454
Point Info Dialog Box
455
Coefficients Dialog Box
455
Verification Setup
456
Time Events Table
457
Time Events
458
Event Description
459
Run Information
463
Open Method File Dialog Box
464
Save Method As Dialog Box
466
Preferences Dialog Box
467
Layout Tab
468
Trace Settings Tab
469
Offsets Tab
471
Colors Tab
472
Fill Peak Table Window
475
Exact View Dialog Box
476
File Menu
477
View Menu
478
Results Menu
479
Edit Method Menu
480
Toolbar Overview
483
Method Quick Link Toolbar
484
Chromatogram Toolbar
484
Locator Window
487
Main Window
488
Opening Data Files
489
Zooming and Scrolling
489
Autoscaling
490
Moving Baselines
490
Info-Panels
491
Cursor Info-Panel
492
Run File Info-Panel
492
Visual Method Edit Window
493
Types of Time Events
494
Right Mouse Menus
496
Action Effect of Action
497
GC Interactive Graphics
499
The Locator Window
500
Changing Viewing Options
503
The Preferences Dialog Box
504
Offsets
505
Selecting a Method
506
Integration Parameters
509
Filling the Peak Table
512
These events are selected
514
Calculating Results
515
Viewing Results
517
Viewing Calibration Curves
518
GC Standard Report Method
521
Results Format
523
Chromatogram Format
524
Print Options
527
Automated Report Generation
530
Select Printer Setup
531
Specify a Print action
532
Select the Data File
534
Method Builder Dialog Boxes
537
Add Password Dialog Box
540
Change Password Dialog Box
541
Star Assistant Wizard
545
Select Configuration
546
Configure Modules
547
Confirm Configuration
550
Method Builder Menus
551
Window Menu
552
Method Builder Toolbars
555
Directory Toolbar
556
Window Toolbar
557
Method Builder Window
559
Method Directory
560
Method Parameters
561
Module Information Editor
563
Creating a Section
564
Deleting a Section
564
Renaming a Section
564
Adding an Entry to a Section
565
Commands
567
Dialog Boxes
568
Security Administration
571
Application Locking
573
File Revision Settings
574
Standard GC Reports Command
577
Options Menu
578
Print Dialog Box
582
Printer Setup Dialog Box
583
Title Dialog Box
583
Results Options Dialog Box
586
Find Dialog Box
587
Standard GC Reports Format
589
Descriptions
589
Verification Report
595
Standard GC Reports Toolbar
597
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